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Research Article

SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL

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Mehmet Ali Özler , Said Nadeem
J Ong Chem Res, 2015, 2 (1), 28-42, DOI: https://doi.org/10.5281/zenodo.23590186, ISSN 2651-4338
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Abstract

A Rh3+ complex 4 derived from 4-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)phenol 3 was prepared at room temperature. 3 was stirred with pentamethylcyclopentadienlyrhodium chloride dimer for 30 minutes which resulted yellow precipitates which were washed with methanol, redissolved in acetone and purified chromatographically with ethanol. Phenanthroline-derived 3 was reacted with (3-chloropropyl)trimethoxysilane to obtain an alkylated compound 5. Silica particles were functionalized by reacting with 5 at 70 oC in DMF for 6 h. Functionalized silica particles can be used for removal of different metals from aqueous and organic solutions and due to their bigger size can be easily filtered.
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The team behind this paper

2 authors, 1 institution.

This paper Teknopark İzmir — Türkiye Teknopark İzmir 1 author Mehmet Ali Özler — corresponding author MÖ Mehmet Ali Özler ✉ Said Nadeem SN Said Nadeem

1 of them has not recorded an affiliation.

Readership

295 reads over 34 months.

February 2024 November 2026

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This article is token #17 of SciMatic Articles (ERC-1155): 1,000,000 tokens, minted once, never more. The chain also stores a fingerprint (SHA-256) of the article's record, so anyone can check that it has not been altered.

HolderWalletTokens
SciMatic 0xc35709…277732 100,000 (10%)
Mehmet Ali Özler 0x802281…D8Ded7 450,000 (45%)
Said Nadeem 0x75286a…bEDc8A 450,000 (45%)
Content hash 0x5b8d21d9dcc805cbfa35f6cee45429b1a2c0d554f455391b912decf27dd8be75
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Bibliographic Information

Mehmet Ali Özler, Said Nadeem, (2015). SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL, Journal of Ongoing Chemical Research, 2(1): 28-42
Bibtex Citation
@article{mehmet_ali_Özler2015jocr,
author = {Mehmet Ali Özler and Said Nadeem},
title = {SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL},
journal = {Journal of Ongoing Chemical Research},
year = {2015},
volume = {2},
number = {1},
pages = {28-42},
doi = {10.5281/zenodo.23590186},
url = {https://scimatic.org/show_manuscript/17}
}
APA Citation
Özler, M.A., Nadeem, S., (2015). SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL. Journal of Ongoing Chemical Research, 2(1), 28-42. https://doi.org/10.5281/zenodo.23590186

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