Research Article
SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL
620
reads
|
Mehmet Ali Özler,
Said Nadeem,
J Ong Chem Res, 2015, 2 (1), 28-42, doi: , ISSN 2651-4338
|
|
|---|---|
|
Abstract:
A Rh3+ complex 4 derived from 4-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)phenol 3 was prepared at room temperature. 3 was stirred with pentamethylcyclopentadienlyrhodium chloride dimer for 30 minutes which resulted yellow precipitates which were washed with methanol, redissolved in acetone and purified chromatographically with ethanol. Phenanthroline-derived 3 was reacted with (3-chloropropyl)trimethoxysilane to obtain an alkylated compound 5. Silica particles were functionalized by reacting with 5 at 70 oC in DMF for 6 h. Functionalized silica particles can be used for removal of different metals from aqueous and organic solutions and due to their bigger size can be easily filtered.
Keywords:
|
|
|
|
Bibliographic Information
Mehmet Ali Özler, Said Nadeem, (2015). SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL, Journal of Ongoing Chemical Research, 2(1): 28-42
Bibtex Citation
@article{mehmet_ali_Özler2015jocr,
author = {Mehmet Ali Özler and Said Nadeem},
title = {SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL},
journal = {Journal of Ongoing Chemical Research},
year = {2015},
volume = {2},
number = {1},
pages = {28-42},
doi = {},
url = {https://scimatic.org/show_manuscript/17}
}
APA Citation
Özler, M.A., Nadeem, S., (2015). SYNTHESIS OF NOVEL NAKED-EYE Fe3+ CHEMOSENSING SILICA PARTICLES AND Rh+3 COMPLEX BASED ON 4-(1H-IMIDAZO[4,5-f][1,10]PHENANTHROLINE-2YLPHENOL. Journal of Ongoing Chemical Research, 2(1), 28-42. https://doi.org/
