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Research Article

ISOLATION OF HIGHLY ACTIVE ANTIRADICAL AND ANTIOXIDANT POLYPHENOLICS FROM PLANT EXTRACTS USING NOVEL POLYMERIC ADSORBENT PARTICLES

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Hüseyin Çiçek , Onur Çetinkaya , Melek Tezcan , Meryem Çiçek , Gökhan Koçak
J Ong Chem Res, 2016, 2 (2), 45-63, ISSN 2651-4338
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Abstract

Boronic acids monomers shows optimum adsorption of diols at pH 8.5. In this study, we were able to reduce this pH to 7.0 by using 4-(N-allylsulfamoil)phenylboronic acid (ASPBA) monomer copolymer. Methacrylate (MA) and our synthesized ASPBA were used to prepare millimeter sized poly(methacrylate-co-4-(N- allylsulfamoil) phenylboronic acid) (poly(MA-co-ASPBA)) particles. These particles were characterized by 1H NMR, FTIR and TGA. The prepared particles were mixed with the extract of Hypericum perforatum L. (centaury) and showed highly selective interaction with the flavonoids. Antioxidant and antiradical compounds were adsorbed over the surface of the particles and later desorbed. These macroporous particles can be used in selective isolation of natural products from plant extracts, especially cis-diols. Our prepared particles can be used as packing materials in the columns to selectively capture the target polyphenolics. Alternatively, the particles can be mixed with the extracts to adsorb the target polyphenolics, and then desorb to obtain selective isolation.
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The team behind this paper

5 authors.

This paper Hüseyin Çiçek — corresponding author HÇ Hüseyin Çiçek ✉ Onur Çetinkaya OÇ Onur Çetinkaya Melek Tezcan MT Melek Tezcan Meryem Çiçek MÇ Meryem Çiçek Gökhan Koçak GK Gökhan Koçak

5 of them have not recorded an affiliation.

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This article is token #25 of SciMatic Articles (ERC-1155): 1,000,000 tokens, minted once, never more. The chain also stores a fingerprint (SHA-256) of the article's record, so anyone can check that it has not been altered.

HolderWalletTokens
SciMatic 0xc35709…277732 100,000 (10%)
Hüseyin Çiçek 0xe891d6…Db47bF 180,000 (18%)
Onur Çetinkaya 0x64bF34…Fa853B 180,000 (18%)
Melek Tezcan 0x0449A8…18a1B6 180,000 (18%)
Meryem Çiçek 0x480138…78dB8B 180,000 (18%)
Gökhan Koçak 0x2A7b4c…CD9c1e 180,000 (18%)
Content hash 0x96ae24f5434930db5bfa9bcdf0470ce6763cd2af45c001701d5fd9ea8128a246
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Bibliographic Information

Hüseyin Çiçek, Onur Çetinkaya, Melek Tezcan, Meryem Çiçek, Gökhan Koçak, (2016). ISOLATION OF HIGHLY ACTIVE ANTIRADICAL AND ANTIOXIDANT POLYPHENOLICS FROM PLANT EXTRACTS USING NOVEL POLYMERIC ADSORBENT PARTICLES, Journal of Ongoing Chemical Research, 2(2): 45-63
Bibtex Citation
@article{hüseyin_Çiçek2016jocr,
author = {Hüseyin Çiçek and Onur Çetinkaya and Melek Tezcan and Meryem Çiçek and Gökhan Koçak},
title = {ISOLATION OF HIGHLY ACTIVE ANTIRADICAL AND ANTIOXIDANT POLYPHENOLICS FROM PLANT EXTRACTS USING NOVEL POLYMERIC ADSORBENT PARTICLES},
journal = {Journal of Ongoing Chemical Research},
year = {2016},
volume = {2},
number = {2},
pages = {45-63},
doi = {},
url = {https://scimatic.org/show_manuscript/25}
}
APA Citation
Çiçek, H., Çetinkaya, O., Tezcan, M., Çiçek, M., Koçak, G., (2016). ISOLATION OF HIGHLY ACTIVE ANTIRADICAL AND ANTIOXIDANT POLYPHENOLICS FROM PLANT EXTRACTS USING NOVEL POLYMERIC ADSORBENT PARTICLES. Journal of Ongoing Chemical Research, 2(2), 45-63. https://doi.org/

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