Research Article

DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO)

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Said Nadeem , Ayhan Sıtkı Demir , İlke Şimşek , Muhammad Raza Shah

J Ong Chem Res, 2014, 1 (3), 107-115, doi: , ISSN 2651-4338

Abstract

The synthesis of dimethyldioxirane (DMD/DMDO) is as complicated as its storage. It should be used within a week after its synthesis. Developments were gained in the synthetic procedure of DMD/DMDO in two steps and enough yield was obtained at moderate temperature compared to literature procedures (-78 ^oC). The dry ice before trap was replaced with a condenser containing chilled methanol which also resulted the condensation of DMD/DMDO back from the vacuum trap. Diethyl formylphosphonate 6 was synthesized by the oxidation of diazomethylphosphonate 5 with DMD/DMDO at different temperatures starting from -78 to 0 ^oC.

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Bibliographic Information

Said Nadeem, Ayhan Sıtkı Demir, İlke Şimşek, Muhammad Raza Shah, (2014). DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO), Journal of Ongoing Chemical Research, 1(3): 107-115

Bibtex Citation


                        
            @article{said_nadeem2014jocr,

                author       = {Said Nadeem and Ayhan Sıtkı Demir and İlke Şimşek and Muhammad Raza Shah},

                title        = {DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO)},

                journal      = {Journal of Ongoing Chemical Research},

                year         = {2014},

                volume       = {1},

                number       = {3},

                pages        = {107-115},

                doi          = {},

                url          = {https://scimatic.org/show_manuscript/119}

              }

APA Citation

Nadeem, S., Demir, A.S., Şimşek, İ., Shah, M.R., (2014). DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO). Journal of Ongoing Chemical Research, 1(3), 107-115. https://doi.org/

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DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO)

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