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Research Article

DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO)

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Said Nadeem , Ayhan Sıtkı Demir , İlke Şimşek , Muhammad Raza Shah
J Ong Chem Res, 2014, 1 (3), 107-115, ISSN 2651-4338
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Abstract

 

The synthesis of dimethyldioxirane (DMD/DMDO) is as complicated as its storage. It should be used within a week after its synthesis. Developments were gained in the synthetic procedure of DMD/DMDO in two steps and enough yield was obtained at moderate temperature compared to literature procedures (-78 oC). The dry ice before trap was replaced with a condenser containing chilled methanol which also resulted the condensation of DMD/DMDO back from the vacuum trap. Diethyl formylphosphonate 6 was synthesized by the oxidation of diazomethylphosphonate 5 with DMD/DMDO at different temperatures starting from -78 to 0 oC.

Authors 4
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The team behind this paper

4 authors, 1 institution.

This paper Teknopark İzmir — Türkiye Teknopark İzmir 1 author Said Nadeem — corresponding author SN Said Nadeem ✉ Ayhan Sıtkı Demir AD Ayhan Sıtkı Demir İlke Şimşek İŞ İlke Şimşek Muhammad Raza Shah MS Muhammad Raza Shah

3 of them have not recorded an affiliation.

Readership

356 reads over 33 months.

February 2024 October 2026

On SciChain

This article is token #119 of SciMatic Articles (ERC-1155): 1,000,000 tokens, minted once, never more. The chain also stores a fingerprint (SHA-256) of the article's record, so anyone can check that it has not been altered.

HolderWalletTokens
SciMatic 0xc35709…277732 100,000 (10%)
Said Nadeem 0x75286a…bEDc8A 225,000 (22.5%)
Ayhan Sıtkı Demir 0x278263…97A0b2 225,000 (22.5%)
İlke Şimşek 0x028B06…964D1a 225,000 (22.5%)
Muhammad Raza Shah 0x181CE8…2Fab5C 225,000 (22.5%)
Content hash 0xb5e35cf57cf36d366f6998f5f0bcb02226797db257556b5f4b719681220567c7
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Bibliographic Information

Said Nadeem, Ayhan Sıtkı Demir, İlke Şimşek, Muhammad Raza Shah, (2014). DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO), Journal of Ongoing Chemical Research, 1(3): 107-115
Bibtex Citation
@article{said_nadeem2014jocr,
author = {Said Nadeem and Ayhan Sıtkı Demir and İlke Şimşek and Muhammad Raza Shah},
title = {DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO)},
journal = {Journal of Ongoing Chemical Research},
year = {2014},
volume = {1},
number = {3},
pages = {107-115},
doi = {},
url = {https://scimatic.org/show_manuscript/119}
}
APA Citation
Nadeem, S., Demir, A.S., Şimşek, İ., Shah, M.R., (2014). DEVELOPMENTS IN THE PREPARATION OF DIMETHYLDIOXIRANE (DMD/DMDO). Journal of Ongoing Chemical Research, 1(3), 107-115. https://doi.org/

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