parameter optimization for sintering of la0.6sr0.4co0.2fe0.8o3-6 (lscf6428) perovskite-structured ceramics by taguchi method
;Hashim Siti Salwa;Bhatia Subhash;Mohamed Abdul Rahman
european romantic review2016Vol. 48pp. 177-189
196
salwa2016scienceparameter
Abstract
The influence of sintering temperature, sintering time and heating rate on
the shrinkage rate, sintered density and porosity of La0.6Sr0.4Co0.2Fe0.8O3-ó
(LSCF6428) perovskite-structured ceramics has been analyzed and the optimum
sintering parameters have been determined by using Taguchi experimental
design method. The analysis of variance (ANOVA) shows that the most
significant parameter is sintering temperature, while the sintering time and
heating rate are the least significant parameters. The optimum sintering
parameter combination within the experimental ranges was found to be 1400°C,
20 h and 10°C/min. The shrinkage rate of 15.97%, the sintered density of 6.06
g/cm³ and the porosity of 0.15% were obtained using these co-optimized
sintering parameters. The SEM micrographs confirm that sintering temperature
has pronounced effect on the densification and porosity reduction of LSCF6428
flat membranes.