crystal structure of 1-methoxy-5-methyl-n-phenyl-1,2,3-triazole-4-carboxamide

crystal structure of 1-methoxy-5-methyl-n-phenyl-1,2,3-triazole-4-carboxamide

;Inna S. Khazhieva;Tatiana V. Glukhareva;Pavel A. Slepukhin;Yury Yu. Morzherin
Disability and rehabilitation 2015 Vol. 71 pp. o798-o798
175
khazhieva2015actacrystal

Abstract

The title compound, C11H12N4O2,was prepared via the transformation of sodium 4-acetyl-1-phenyl-1H-[1.2.3]triazolate under the action of methoxyamine hydrochloride. The dihedral angle between the triazole and phenyl rings is 25.12 (16)° and the C atom of the methoxy group deviates from the triazole plane by 0.894 (4)Å. The conformation of the CONHR-group is consolodated by an intramolecular N—H...N hydrogen bond to an N-atom of the triazole ring, which closes an S(5) ring. In the crystal, weak N—H...N hydrogen bonds link the molecules into C(6) [010] chains.

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