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Research Article

SNYTHESIS AND CHARACTERIZATION OF HYDRATED TRIS (2, 2'- BIPYRIDINE) DICHLORIDE RUTHENIUM (II) COMPLEX AND ITS ELECTROCATALYTIC ACTIVITY TOWARDS CARBON DI OXIDE REDUCTION

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Asghar Khan , Ho Shik Won
J Ong Chem Res, 2014, 1 (3), 83-97, ISSN 2651-4338
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Abstract

A new convenient method for the synthesis of hydrated tris (2, 2'-bipyridine) dichloride ruthenium (II) complex has been developed. We introduced the chlorosulfonic acid as a chlorinating reagent during our synthetic process which replace the hexafluorophosphate radical of the [Ru (bpy) 3] (PF6)2 complex with chloride, form hydrated Tris [Ru (bpy) 3] (Cl)2 complex. The corresponding complex is characterized with UV-Visible, IR, CV, 1 H and C 13 NMR spectroscopic technique. The synthesized hydrated ruthenium complex was then checked as an electrocatalyst for the reduction of carbon dioxide in a designed electrolytic cell. The carbon dioxide gas in the aqueous solution of Tris (2, 2'-bipyridine) ruthenium (II) dichloride catalyst, at the potential of 1.5 V reduced to methane gas, examined with FTIR spectrometer.

Keywords Chlorosulfonic acid 2,2'-bipyridine Spectroscopic study Cyclic voltammetry Electrocatalytic reduction
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The team behind this paper

2 authors.

This paper Asghar Khan — corresponding author AK Asghar Khan ✉ Ho Shik Won HW Ho Shik Won

2 of them have not recorded an affiliation.

Readership

400 reads over 33 months.

February 2024 October 2026

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This article is token #111 of SciMatic Articles (ERC-1155): 1,000,000 tokens, minted once, never more. The chain also stores a fingerprint (SHA-256) of the article's record, so anyone can check that it has not been altered.

HolderWalletTokens
SciMatic 0xc35709…277732 100,000 (10%)
Asghar Khan 0x5e5B47…dbda97 450,000 (45%)
Ho Shik Won 0x9422b8…173fF1 450,000 (45%)
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Bibliographic Information

Asghar Khan, Ho Shik Won, (2014). SNYTHESIS AND CHARACTERIZATION OF HYDRATED TRIS (2, 2'- BIPYRIDINE) DICHLORIDE RUTHENIUM (II) COMPLEX AND ITS ELECTROCATALYTIC ACTIVITY TOWARDS CARBON DI OXIDE REDUCTION, Journal of Ongoing Chemical Research, 1(3): 83-97
Bibtex Citation
@article{asghar_khan2014jocr,
author = {Asghar Khan and Ho Shik Won},
title = {SNYTHESIS AND CHARACTERIZATION OF HYDRATED TRIS (2, 2'- BIPYRIDINE) DICHLORIDE RUTHENIUM (II) COMPLEX AND ITS ELECTROCATALYTIC ACTIVITY TOWARDS CARBON DI OXIDE REDUCTION},
journal = {Journal of Ongoing Chemical Research},
year = {2014},
volume = {1},
number = {3},
pages = {83-97},
doi = {},
url = {https://scimatic.org/show_manuscript/111}
}
APA Citation
Khan, A., Won, H.S., (2014). SNYTHESIS AND CHARACTERIZATION OF HYDRATED TRIS (2, 2'- BIPYRIDINE) DICHLORIDE RUTHENIUM (II) COMPLEX AND ITS ELECTROCATALYTIC ACTIVITY TOWARDS CARBON DI OXIDE REDUCTION. Journal of Ongoing Chemical Research, 1(3), 83-97. https://doi.org/

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