Photo-induced glycosylation using a diaryldisulfide as an organo-Lewis photoacid catalyst.
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Photo-induced glycosylation using a diaryldisulfide as an organo-Lewis photoacid catalyst.

Iibuchi, Naoto;Eto, Takahiro;Aoyagi, Manabu;Kurinami, Reiji;Sakai, Hayato;Hasobe, Taku;Takahashi, Daisuke;Toshima, Kazunobu;
Organic & biomolecular chemistry 2020
192
iibuchi2020photoinducedorganic

Abstract

Photo-induced glycosylations of several acceptors with trichloroacetimidate donors using bis(2-naphthyl)disulfide as an organo-Lewis photoacid (LPA) catalyst proceeded effectively to give the corresponding glycosides in good to high yields. In addition, the ground and excited state absorption spectra of bis(2-naphthyl)disulfide with or without NEt3 suggested the Lewis acidity of bis(2-naphthyl)disulfide upon photo-irradiation.

Keywords

copper catalysis * c-h arylation * heterogeneous catalysis * hybrid catalysis * photocatalysis

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DOI:
10.1039/c9ob02674f

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ID: 81570
Ref Key: iibuchi2020photoinducedorganic
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