Solvent-controlled selective synthesis of biphenols and quinones via oxidative coupling of phenols.
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Solvent-controlled selective synthesis of biphenols and quinones via oxidative coupling of phenols.

More, Nagnath Yadav;Jeganmohan, Masilamani;
Chemical communications (Cambridge, England) 2017 Vol. 53 pp. 9616-9619
219
more2017solventcontrolledchemical

Abstract

A regioselective synthesis of unsymmetrical and symmetrical biphenols and binaphthols via oxidative coupling of phenols or naphthols in the presence of KSO in CFCOOH under ambient conditions is described. Interestingly, the 1 : 1 ratio of HO and CHCN solvent mixtures at 80 °C instead of CFCOOH provided substituted unsymmetrical quinones. A gram-scale synthesis of biphenols and binaphthols was demonstrated.

Keywords

antioxidants nos2 ho-1 cox-2 raw264.7 cells eugenol-related compounds theoretical parameters

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DOI:
10.1039/c7cc04829g

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ID: 263122
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