development of one-pot three component reaction for the synthesis of n′-aryl-n-cyanoformamidines, essential precursors of formamidine pesticides family
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development of one-pot three component reaction for the synthesis of n′-aryl-n-cyanoformamidines, essential precursors of formamidine pesticides family

;Antonio De Nino;Loredana Maiuolo;Monica Nardi;Raffaele Pasceri;Antonio Procopio;Beatrice Russo
Behavioural brain research 2016 Vol. 9 pp. 32-37
154
nino2016arabiandevelopment

Abstract

Efficient one-pot three component reaction of aniline derivatives with cyanoamide and triethyl orthoformate at reflux in toluene affords N′-aryl-N-cyanoformamidines in high yields just by the distillation of the azeotrope toluene/ethyl alcohol. Labelled d9-Amitraz is prepared by the application of this procedure in the synthesis of formamidine pesticides family.

Keywords

pesticides

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DOI:
10.1016/j.arabjc.2015.06.016
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http://www.sciencedirect.com/science/article/pii/S...

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ID: 259364
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