batch and continuous flow preparation of hantzsch 1,4-dihydropyridines under microwave heating and simultaneous real-time monitoring by raman spectroscopy. an exploratory study
Abstract
Dialkyl 1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylates have been prepared in a batch mode under conventional heating as well as under continuous flow conditions in the Miniflow 200SS, Sairem’s microwave-assisted batch and continuous flow equipment. Real-time monitoring of the reactions by Raman spectroscopy enabled to compare both heating modes and to determine (optimized) reaction times.
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241742
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0x95644003c57E6F55A65596E3D9Eac6813e3566dA
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241742
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10.3390/molecules19079986
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Scimatic Chain (ID: 481)
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