2ii-vii, 3i-vii, 6i-vii-icosa-o-acetyl-2i-deoxy-cyclomaltoheptaose
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2ii-vii, 3i-vii, 6i-vii-icosa-o-acetyl-2i-deoxy-cyclomaltoheptaose

;Atsushi Miyagawa;Kazuki Kano;Aya Yoshida;Hatsuo Yamamura
journal of chemical sciences 2016 Vol. 2016 pp. M900-
100
miyagawa2016molbank2ii-vii,

Abstract

Deoxygenation of a secondary hydroxy group on β-cyclodextrin was conducted to prepare the title compound 2II-VII, 3I-VII, 6I-VII-icosa-O-acetyl-2I-deoxy-cyclomaltoheptaose. The synthetic procedure comprised a two-step reaction—phenoxythiocarbonylation and Barton-McCombie deoxygenation. The synthesized compound was characterized by 1H-NMR, 13C-NMR, HRMS, and elemental analysis.

Keywords

cyclodextrin barton-mccombie deoxygenationinorganic chemistry

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DOI:
10.3390/M900
URL:
http://www.mdpi.com/1422-8599/2016/2/M900

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ID: 140617
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