Total Synthesis of Dactylicapnosines A and B.

Total Synthesis of Dactylicapnosines A and B.

Zhao, Yinjiao;Li, Yuda;Wang, Bei;Zhao, Jingfeng;Li, Liang;Luo, Xiao-Dong;Zhang, Hongbin;
The Journal of organic chemistry 2020
96
zhao2020totalthe

Abstract

Dactylicapnosines A and B, two natural products from , exhibited potent anti-inflammatory and analgesic activities both in vitro and in vivo. In this paper, we report our second-generation synthesis of dactylicapnosine A and the first total synthesis of dactylicapnosine B. Our synthetic route features acid-induced isomerization of -quinone (), Co-mediated regioselective ring contraction of -quinone (), and oxidative methoxylation of enone (). This modified sequence provides dactylicapnosine A in 14 steps with an overall yield of 12% from a known compound () and also offers opportunities to synthesize dactylicapnosine-like analogues for biological investigations.

Citation

ID: 189306
Ref Key: zhao2020totalthe
Use this key to autocite in SciMatic or Thesis Manager

References

Blockchain Verification

Account:
NFT Contract Address:
0x95644003c57E6F55A65596E3D9Eac6813e3566dA
Article ID:
189306
Unique Identifier:
10.1021/acs.joc.0c01900
Network:
Scimatic Chain (ID: 481)
Loading...
Blockchain Readiness Checklist
Authors
Abstract
Journal Name
Year
Title
5/5
Creates 1,000,000 NFT tokens for this article
Token Features:
  • ERC-1155 Standard NFT
  • 1 Million Supply per Article
  • Transferable via MetaMask
  • Permanent Blockchain Record
Blockchain QR Code
Scan with Saymatik Web3.0 Wallet

Saymatik Web3.0 Wallet