caracterização da pureza de fosfatidilcolina da soja através de rmn de ¹h e de 31p characterization of soybean phosphatidylcholine purity by ¹h and 31p nmr
Current Language EN
English English Türkçe Türkçe Español Español Português Português Pусский Pусский Filipino Filipino Tiếng Việt Tiếng Việt हिन्दी हिन्दी العربية العربية বাংলা বাংলা Deutsch Deutsch 中文 中文

caracterização da pureza de fosfatidilcolina da soja através de rmn de ¹h e de 31p characterization of soybean phosphatidylcholine purity by ¹h and 31p nmr

;Omar Mertins;Marcelo Sebben;Paulo Henrique Schneider;Adriana Raffin Pohlmann;Nádya Pesce da Silveira
greece and rome 2008 Vol. 31 pp. 1856-1859
220
mertins2008qumicacaracterizao

Abstract

A strategy is proposed to evaluate the purity of phosphatidylcholine from soybean lecithin, obtained by extraction or column chromatography, using the integrals ratio of ¹H NMR spectra. Integrals of methylene signals, around 1.3 and 1.6 ppm, are added and divided by the integral of the choline methyl groups, around 3.3 ppm. Before purification, a ratio of 19.68±1.37 was determined. Using extraction, a ratio of 10.70±0.61 was found, while from column chromatography, a value of 2.99±0.25 was detected. 31P NMR of standard phosphatidylcholine showed signals at -0.2 and -0.9 ppm, whereas the purified one showed a single signal at -0.9 ppm.

Keywords

NMR phosphatidylcholine

Access

DOI:
10.1590/S0100-40422008000700043
URL:
http://www.scielo.br/scielo.php?script=sci_arttext...

Citation

ID: 134206
Ref Key: mertins2008qumicacaracterizao
Use this key to autocite in SciMatic or Thesis Manager

References

References

No Bibliography

Blockchain Verification

Account:
NFT Contract Address:
0x95644003c57E6F55A65596E3D9Eac6813e3566dA
Article ID:
134206
Unique Identifier:
10.1590/S0100-40422008000700043
Network:
Scimatic Chain (ID: 481)
Blockchain Readiness Checklist
Authors
Abstract
Journal Name
Year
Title
5/5
Creates 1,000,000 NFT tokens for this article
Token Features:
  • ERC-1155 Standard NFT
  • 1 Million Supply per Article
  • Transferable via MetaMask
  • Permanent Blockchain Record
Blockchain QR Code
Scan with Saymatik Web3.0 Wallet
Gas fees required in SCI Coins
Buy SCI

Saymatik Web3.0 Wallet

Google Play
App Store